Studies on Synthesis and Characterization of Advanced Electrode Material Nanocomposite of Tetra Metal Oxides of Fe-Mn-Ni-Co-ZIF-8@rGO

Authors

A. Niresha Gnana Mary

PhD Scholar, PG & Research Department of Chemistry, St. Joseph’s College (Affiliated to Bharathidasan University), Tiruchirappalli-2, Tamil Nadu (India)

Dr. A. S. Stella Shalini

Associate Professor, PG & Research Department of Chemistry, St. Joseph’s College(Affiliated to Bharathidasan University), Tiruchirappalli-2, Tamil Nadu (India)

Dr. G. Sivasankari

Assistant Professor, PG & Research Department of Chemistry, Cauvery College,(Affiliated to Bharathidasan University), Tiruchirappalli-18, Tamil Nadu (India)

Article Information

DOI: 10.51584/IJRIAS.2026.11060161

Subject Category: Nano chemistry

Volume/Issue: 11/6 | Page No: 2142-2151

Publication Timeline

Submitted: 2026-06-15

Accepted: 2026-06-20

Published: 2026-07-04

Abstract

The growing demand for efficient and sustainable energy storage systems has accelerated the development of advanced electrode materials for high-performance supercapacitors. In this study, novel nanocomposite electrodes based on zeolitic imidazolate framework-8, Fe-Mn-Ni-Co tetra-metal oxides and reduced graphene oxide were designed, synthesized and characterized to enhance electrochemical energy storage performance. The synthesized materials were systematically characterized using Fourier Transform Infrared Spectroscopy and X-ray Diffraction techniques. FTIR analysis confirmed the coexistence of characteristic organic functional groups of ZIF-8 and metal-oxygen vibrations of transition metal oxides, indicating successful hybrid composite formation. XRD studies revealed the crystalline nature and phase purity of ZIF-8 along with the formation of nanocrystalline Fe-Mn-Ni-Co oxide structures. The presence of multiple transition metal ions generated lattice distortions and increased the density of electroactive sites, thereby facilitating enhanced redox reactions. Overall, the study demonstrates that ZIF-8-derived Fe-Mn-Ni-Co oxide/rGO nanocomposites are promising electrode materials for next-generation supercapacitors

Keywords

Tetra-metal oxides, Fe-Mn-Ni-Co oxide, Reduced graphene oxide (rGO), Nanocomposites, Energy storage, Electrochemical performance

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